Abstract.
Solid State Ionics 203 (2011) 52–56. (DOI: 10.1016/j.ssi.2011.09.010).
The preparation of nano-sized BaCeO3 powder using starch as a polymerization agent is described herein. Phase evolution during the decomposition process of a (BaCe)-gel was monitored by XRD. A phase-pure nano-sized BaCeO3 powder was obtained after calcining of the (BaCe)-gel at 920 °C. The resulting powder has a specific surface area of 15.4m2/g. TEM investigations reveal particles mainly in the size range of 30 to 65 nm. The shrinkage and sintering behaviour of resulting powder compacts were studied in comparison to a coarse-grained mixed-oxide BaCeO3 powder (SBET = 2.1 m2/g). Dilatometric measurements show that the beginning of shrinkage of compacts from the nano-sized powder is downshifted by 300 °C compared to mixed-oxide powder. Compacts from the nano-sized powder reach a relative density of 91 % after sintering at 1450 °C for 10 h.
Koferstein, R. (2021). Synthesis and Characterization of a Nano-scaled Barium Cerate Perovskite Powder Using Starch as Polymerization Agent. Afribary. Retrieved from https://afribary.com/works/synthesis-and-characterization-of-a-nano-scaled-barium-cerate-perovskite-powder-using-starch-as-polymerization-agent
Koferstein, Roberto "Synthesis and Characterization of a Nano-scaled Barium Cerate Perovskite Powder Using Starch as Polymerization Agent" Afribary. Afribary, 02 Aug. 2021, https://afribary.com/works/synthesis-and-characterization-of-a-nano-scaled-barium-cerate-perovskite-powder-using-starch-as-polymerization-agent. Accessed 23 Apr. 2024.
Koferstein, Roberto . "Synthesis and Characterization of a Nano-scaled Barium Cerate Perovskite Powder Using Starch as Polymerization Agent". Afribary, Afribary, 02 Aug. 2021. Web. 23 Apr. 2024. < https://afribary.com/works/synthesis-and-characterization-of-a-nano-scaled-barium-cerate-perovskite-powder-using-starch-as-polymerization-agent >.
Koferstein, Roberto . "Synthesis and Characterization of a Nano-scaled Barium Cerate Perovskite Powder Using Starch as Polymerization Agent" Afribary (2021). Accessed April 23, 2024. https://afribary.com/works/synthesis-and-characterization-of-a-nano-scaled-barium-cerate-perovskite-powder-using-starch-as-polymerization-agent