ABSTRACT Oxygen absorption studies of blends of oils of seed s eed melon~(~SD), rubber (RSO) and linseed (LSD) have been L carried out at room temperature in order to optimise the drying performance of MSO and RSO. A manometer was used to measure O2 absorbed. The set-to-touch time ( STTT) of o i l o r o i l blend was measured after 3 hours of O2 absorption and 18 hours of ageing. Addition of LSO to MSO reduced its STTT from 12.25 hours to 4.0 hours at 50/50; this compares favourably with the ...
ABSTRACT The study investigated the nutrients and phytochemical compositions of some leafy vegetables in Nigeria (Hibiscus cannabinus, Adansonia digitata, Sesamum indicum and Cassia tora leaves) and the effects of their extracts on blood glucose and lipid profile of alloxan induced diabetic rats. Two kilogrammes of each of the vegetables were bought fresh, sorted by removing extraneous material, washed with deionized water and separately pulverized using Gallenkamp mixer Kenwood –MPR 201. A...
Abstract-The Ishiagu lead-zinc deposits of southeastern Nigeria are associated with folded shales of the Asu River Group. The PbZn mineralization is restricted to a series of closely spaced, steeply dipping subparallel fractures which trend NW-SE and typically form en-echelon patterns. Along a second set of fissures, oriented NE-SW and of an earlier generation than the NW-SE system, only the gangue minerals (siderite and quartz) are characteristic. The style of mineralization is exclusively f...
ABSTRACT 2-[(E)-[3-[(E)-(2-hydroxyphenyl)methyleneamino]phenyl]iminomethyl]phenol was synthesized from the condensation reaction of 1,3-diaminobenzene and 2-hydroxyzaldehyde in dimethylformaldehyde (DMF). Its coordination characteristic with vanadium(III) and vanadium(V) complexes was studied via, UV/Visible, IR and NMR spectroscopy; stoichiometric, melting point and conductivity determinations. The analytical data of these complexes and the mode of bonding show that, the ligand acted as a te...
ABSTRACT The active drug content and weight uniformity of five brands (A – E) of Amoxicillin Trihydrate capsules in Nsukka open drug market were evaluated to ascertain their quality assurance using UV visible spectroscopy and gravimetry. This study has shown that all the brands analyzed showed significant variations with respect to active drug content determination for the three brands B, D and E. Using United State Pharmacopoeia (USP) and British Pharmacopoeia (BP) specifications of 90 –...
ABSTRACT This work studied the effect of the binary and ternary combinations of pine needle (Pinus pinaster ) dust and bambara nut (Vigna subterranea) chaff with coal dust for briquette production. Briquettes of 100% of the pure coal and the biomass were produced first. The ratios for the blending were as follows 1:1 for the binary combination of each biomass with coal and with themselves, and 1:1:1 for the ternary combination of the two biomass with coal. The feed stocks were dried to a mois...
ABSTRACT Modification of coconut (Cocos nucicera L.) shell activated carbon with an Azo ligand: 1, 2– dihydro-1,5-dimethyl-2-phenyl-4-(E)–(2,3,4-trihydrophenyl)-3H-pyrazol-3-one (DDPTP) and its potentials for the removal of Cd2+, Pb2+ and Ni2+ from polluted water samples were studied. It was activated chemically using CaCO3 as the activating agent. Proximate analysis on the coconut shell showed 8.7 % moisture content, 10.4 % volatile matter, 3.2 % ash content and 77.7 % fixed carbon. The ...
ABSTRACT “A Library is a repository of various forms of recorded information, as well as a collection of data in many formats.” (Metu A. 1987). The design proposal is a consequence of an investigation into the emerging concern about energy efficiency of buildings, the recent advances in information technology and their attending consequences on the planning and architecture of the future library. Demographic data and an understanding of the development need of the growing population valid...
Abstract Suppose that E is a real Banach space .which is both uniformly convex and q-uniformly smooth and that T is a Lipschit;: pseudocontractive self-mapping of a closed convex and bounded subset K of E. Suppose F(T) dcnotes the set of fixed points of T and U denot :s the sunny nonexpansive retraction of K onto F(T) and w any point of K, it is proved that the sequence {xn),"Lo generated from an arbitrary xo E K bv (where I denotes the identity operator on E and {a,),"==, and {Pn),"=o are re...
ABSTRACT The synthesis and characterization of five new linear diazaphenoxazine compounds is reported. The key intermediate, 3-chloro-1-9-diazaphenoxazine, was prepared via a base catalyzed reaction of 2-amino-3-hydroxypyridine with 2,3,5-trichloropyridine in aqueous 1, 4-dioxane. Five 3-amino derivatives of the key intermediate were prepared via Buchwald – Hartwigamination coupling reaction between 3-chloro-1,9-diazaphenoxazine and various heterocyclic amines, under the catalytic influence...
CONTENTS .- - CERTIFICATION: DEDICATION : ABSTRACT ACKNOWLEDGEMENT CHAPTER ONE: INTRODUCTION : ' 1.1 Motivation behind growth of thin Films 1.2 What are thin films .I "3 Uses of thin films 1.4 Deposition techniques : 1.5 Reasons for the technique used in experimentation 10 - CHAPTER TWO : BASIC SEMICONDUCTOR PHYSICS 12 - 39 2.1 What are SemicondLlcrors 12 2.2 Examples of Semiconductors 14 2 '3 Types of Semiconductors 16 2.4 Semiconductor Statistics 20 2 -41 Probability of occupation of allowe...
ABSTRACT Tandem amidation catalyzed synthesis of linear diazaphenoxazine carboxamide derivatives is reported. This was achieved by the reaction of 2-amino-3-hydroxypyridine and 2,3,5-trichloropyridine in aqueous basic medium which gave 3-chloro-1,9-diazaphenoxazine as white solid crystals. 3-Chloro-1,9-diazaphenoxazine was then subjected to Buchwald-Hartwig amidation coupling reaction with various amides namely formamide, phthalamide, 4- nitrobenzamide, benzamide and acetamide via water promo...
ABSTRACT Synthesis of twelve O-arylated diazabenzo[a]phenoxazine-5-one and its carbocyclic analogue is reported in 46 - 99 % yields. The intermediates were prepared by anhydrous base catalyzed reaction of 2,3-dichloro-1,4- naphthoquinone with 4,5-diamino-6-hydroxyl-2-mercaptopyrimidine and 2- aminophenol. The O-arylation process occurred smoothly in non-polar solvent, toluene with the inexpensive base, K2PO4 at 110o C. The intermediates were combined with a variety of electron-deficient, elec...
ABSTRACT Resistivity surveys were carried out at seven stations within the university of Nigeria, Nsukka and its environs. The objective was to determine areas suitable for the drilling of boreholes for groudhvater. The results generated from this survey were interpreted in terms of the number of subsurface layers, usurer thickness, depth to uquifer and, probable lithology$orrnations. However, lithologic interpretations were carried out using exist ring borehole data from the area. A BEM Terr...
ABSTRACT The study sought to assess the solid waste disposal pattern of sellers in Mile One Market Port Harcourt in order to: identify the solid waste disposal habits of sellers, determine the frequency of clearing dumpsters from the market, determine accessibilityof waste dumpsters to market sellers and ascertain if the pattern of waste disposal significantly vary from different section of the markets.Data wereobtained throughinterviews, questionnaires and on the spot observation. A total of...